2-[(10-bromodecyl)oxy]tetrahydro-2H-pyran | CAS:51795-88-1
2-[(10-bromodecyl)oxy]tetrahydro-2H-pyran
- 名称：2-[(10-溴癸基)氧基]四氢-2H-吡喃 | 2-[(10-bromodecyl)oxy]tetrahydro-2H-pyran
- CAS号：51795-88-1
- 别名：
- 分子式：C15H29BrO2
- 分子量：321.29
- EINESC号：
产品描述
Description for Route of Synthesis:
1. Add toluene and 1,10-decanediol to a three-neck flask, then add 40% hydrobromic acid and stir the mixture at room temperature for 18 hours.
2. Under 0℃ conditions, add p-toluenesulfonic acid monohydrate to the crude product obtained above in a solution of dihydropyran in dichloromethane. Slowly heat the resulting reaction mixture to room temperature and stir overnight; then add water to quench the reaction.
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