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4-Chloropyrrolo[2,3-d]pyrimidine | CAS:3680-69-1

4-Chloropyrrolo[2,3-d]pyrimidine

名称：4-氯吡咯并嘧啶; 4-氯吡咯并[2,3-d]嘧啶; 6-氯-7-脱氮嘌呤 | 4-Chloropyrrolo[2,3-d]pyrimidine
CAS号：3680-69-1
别名：4-Chloro-1H-pyrrolo[2,3-d]pyrimidine; 6-Chloro-7-deazapurine
分子式：C6H4ClN3
分子量：153.57
EINESC号：

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Alfa-Aesar	浏览或下载
Sigma-Aldrich	浏览或下载
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产品合成路线

名称	CAS号
CP 690550	477600-75-2	查看

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同行评议文献

Syndiospecific living polymerization of 4-methylstyrene and styrene with (trimethyl) pentamethylcyclopentadienyltitanium/tris (pentafluorophenyl) borane/trioctylaluminum catalytic system. Kawabe M and Murata M. Journal of Polymer Science Part A: Polymer Chemistry, 39(21), 3692-3706 (2001) An efficient palladium-catalyzed Heck coupling of aryl chlorides with alkenes. Yi C and Hua R. Tetrahedron Letters, 47(15), 2573-2576 (2006) Synthesis and study of cationic, two-coordinate triphenylphosphine-gold-π complexes.Rachel E M Brooner et al.Chemistry (Weinheim an der Bergstrasse, Germany), 19(25), 8276-8284 (2013-04-18) Mercapturic acid metabolites from 2-, 3-, and 4-ethenyl-methylbenzenes in the rat.T Kühler Xenobiotica; the fate of foreign compounds in biological systems, 14(5), 417-428 (1984-05-01) Origin of threefold symmetric torsional potential of methyl group in 4-methylstyrene.Rajeev K Sinha et al.The Journal of chemical physics, 124(14), 144316-144316 (2006-04-22)

备注

Description for route of synthesis: Add 4-hydroxypyrrolo [2,3-d] pyrimidine to excess phosphorus oxychloride, heat to reflux for chlorination reaction, and convert hydroxyl groups into chlorine atoms; After the reaction is complete, excess phosphorus trichloride is removed under reduced pressure. The residue is slowly poured into ice water, neutralized to neutrality with sodium bicarbonate, extracted with ethyl acetate, washed, dried, concentrated, and purified by recrystallization or distillation to obtain the target product 4-chloropyrrolopyrimidine.

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名称	CAS号
CP 690550	477600-75-2	查看

产品描述

物理化学性质

安全数据

SDS

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